Close balance doors, if applicable, to reduce draft. Officer concerned department is responsible for monthly calibration. This sop is applicable to the trolley balance in the department at the plant. The standard operating procedure is applicable to in process quality assurance areas. Take the standard weights of different capacity based on the capacity of the balance as. Clean balance pan after each use with a soft brush or damp towel. Sartorius analytic balance mn 1712mp8 operating manual version.
The precision of the balance should be verified by weighing at least 5 times a weight that is equivalent to approximately 50% of the maximum capacity of the balance. If it is not, press the lbkg key on the keyboard face. The same weight should always be used in these verifications. If any of the observation is out of limit, correct and reset the balance. Before leaving balance the close the glass drafts properly and rezero the balance by pressing. Sop for operation and calibration of mettler toledo. Indicates the message appearing in the balance display. This sop describes the proper operation of the mettler toledo ab2045 analytical balance in the sobran animal facility. Allow to stabilize for 15 to 20 seconds and then select the weight for calibration. Zero tare timing change function page 7 zero point, and taring various weighing methods. Check that the balance and pans are always kept clean. How to examine the repeatability of the balance in routine testing. Calibration balance a wide selection of ultramicro, micro, analytical and precision balances allows you to choose any entrylevel to highperformance balance.
Pick up the checkweight with a forceps, place it carefully on the balance pan, and weigh it. The balance would do internal calibration automatically, give out the print. Sop for operation and calibration of mettler toledo analytical. Retrieve the calibration weight from the inside of the balance.
Repeat the intermediate weighing of the weight cart as if multiple weights were being verified. Ensure that balance is kept on a shockproof bench top. Anthropometric standardization reference manual by timothy g. If the instrument is not used according to the manufacturers operating instructions part 1, part 2 and part 3, protection of the instrument may be impaired. Weight is measured with a calibrated, electronic digital scale or beam balance. Indicates the step number in a procedure or a sequence of changes in the balance display. The 31 weighing design provides two methods of checking the validity of the measurement using an integrated ftest to monitor the. It should be emphasised that the daily checks do not obviate the need to check correct operation of the balance each time weighing is carried out. Check that the balance is placed in a draughtfree area and that the pointer is able to swing freely. In cases where calibration is being performed by the balance user, two test weights with a defined mass will be required. If possible, set the balance to read to 5 decimal places. Routine testing of balances general basic rules for handling balances before using a balance, make sure the balance was left on power for a sufficient period of time mentioned in the balance operating instructions. Check for batteries for battery operated balances to ensure accurate display and functionality.
Purpose of this sop for operation, cleaning, verification, and calibration of bin lifting trolley with weighing balances. The specific sop for the double substitution procedure for each balance is to be followed. Place identical pieces of greaseproof paper on both pans, if the material to be weighed is a greasy material. Verification of the balance is performed by placing a suitable weight depending on the type of balance in the center of the weighing pan once and comparing the result with predefined acceptance criteria.
Clean up any spillage near by balance and on the balancemounting base by soft brush. Equipped with a touch screen, it is also suitable for customised workflows qapps. It is designed to instruct laboratory personnel on how to proceed for thorough cleaning of a balance. Qc for analytical balances wisconsin department of. Standard operating procedures sops for balance testing. Before calibrating the balance, clean the weighing platforms. A satisfactory way of carrying this out is to check the balance for free swing at the tare and loaded position. If all the parameters fall with the acceptance criteria limit, affix the calibration tag no. This is not a calibration of the balance, it is a verification of calibration. To outline the procedure for operation of analytical balances in the traces centre and the. Sop 8 or sop 4 to determine the conventional mass value of the weight cart. Usp chapter 41 weights and balances has been revised recently in 20 for repeatability and accuracy of weighing balances this usp chapter 41 makes it mandatory for pharmaceutical manufacturers to use use a test weight between 5%.
The analytical balance is used when weighing small items such as test articles during formulation and animal organs during necropsy. Weighing by single substitution using a single pan mechanical balance, a full electronic balance, or a balance with digital indications and built in weights may 2019 job aids. Before weighing any filters, verify balance performance by weighing a nist traceable calibration weight 100. Use a mild detergent, di water and lint free wipe if necessary. Man100 weighing equipment checking and calibration. Good weighing practice for lab and production balance. These revisions aim to ensure weighing accuracy and. Sop on procedure for operation of analytical balance. Follow good laboratory practices such as properly exercising the balance prior to calibration.
This demand specifies the usable weighing range of the. Systematic balance testing minimizes risks and reduces costs. Title calibration and maintenance of weigh balances. Auto tare function page 7 i want to tare the balance without waiting for the stability mark to light up. Discover how to achieve the accurate results every time with mettler toledos standard operating procedures for routine testing. Weighing scale calibration how to calibrate weighing.
Officer production is responsible for verification. Operation and cleaning of electronic weighing balance generation of shipper label pallet label for track and trace system using bar code technology as per sscc code following gsi global standards batch packing. Free standard operating procedures consist testing information for lab microbalance, analytical or precision balance on different topics. Using balances the primary method that you will use to measure the amounts of chemicals is to weigh themthat is, to determine their mass. Reference weight set range of 1g to 50g and individual reference weights 1 mg, 10 mg, 100 mg, 100 g, 500 g, 1 kg, 2 kg. For mass production balance, balance sensitivity and eccentricity are major factors for consideration. Analytical balances select a checkweight of an appropriate mass to examine an analytical balance. This procedure is applicable for balance installed in the quality control department. Check the balance leveling gauge to make sure bubble is inside the target. The purpose of the weighing test is to test the accuracy calibrate of the weighing instrument throughout its whole range in several steps, with increasing and decreasing weight.
After resetting, calibrate again all the parameters as mentioned in point 6. Switch on the main power supply to balance and printer. Operating instructions excellence analytical balances xs. Before performing weighing assure that, balance is calibrated. Download as docx, pdf, txt or read online from scribd. Suggested process for verifying analytical balance accuracy and performance 1. According to the current usp chapter 41, the repeatability part of the test defines the starting point of a balances operating range, which is limited to the maximum capacity of the balance and begins at the point at which the balances repeatability is less than or equal to 0. Select a weighing device of a lesser capacity for small. To lay down a procedure for calibration of weighing balances.
The samples are weighed using an appropriate weighing container weighing paper. With more than 140 years of experience and quality made in germany, we offer the best weighing option by excelling in speed, repeatability and accuracy. This sop describes the optimal use and maintenance of a laboratory balance, used to. There are many types of laboratory balance but this procedure focuses on electromagnetic balances. Before weighing the first sample of the day, verify the functionaccuracy of the balance by weighing the precision scale weights 1mg, 10mg, and 50mg. Balance nonlinearity is a less dominant factor for small mass weighing. Do not use the weighing device for loads less than ten percent of the capacity of the range in use.
Us environmental protection agency office of pesticide. Place weighing container on the balance weighing pan. The balance is again in the weighing mode and ready for operation. The procedure is operated by trained members of the group who are deemed competent by the operational area manager, metabolic studies. Sop on calibration of weighing balance pharmastate blog. Enter the each weighing process in balance log book. If using an electronic balance, allow to warm up for at least 60 minutes. Check the level of balance using built in level indicator. Level the balance, most balances have a stand that is adjustable to meet the proper level, use the bubble as a guide. Sop on receipt of raw materials and packaging materials. The latest revisions to the united states pharmacopeia usp general chapters balances and weighing on an analytical balance became official on dec.
Set the standard weights for various balances based on the capacity of the balance as mentioned in table i. This sop describes the optimal use and maintenance of a laboratory balance, i. If the standard deviation obtained is less than ing range and meets the requirements defined for 0. This sop describes the procedure for cleaning a laboratory bench top balance both analytical balance and precision balance. In such case, measuring result should be corrected according to.
List of standard operating procedure sops in production. California environmental protection agency air resources. You may use this feature by adding opto modules and additional hardware to control filling or loading of cars. Auto zero function page 7 i want to automatically tare the balance set the display to zero after outputting a weight reading. Standard operating procedure to evaluate the performance of analytical balance used for the analysis in. Carefully clean the weighing scale, most weighing scale pans can be removed for better cleaning. Used to measure the weight of objects in the laboratory, such as media and reagent ingredients and disinfectant containers. Standard operating procedure operation of analytical balances. Your balance must provide the same result for repeated weighing of the same load under the same measurement conditions. If during or before weighing power supply fails, then recalibrate the balance.
1000 154 1518 200 801 502 1463 368 1457 845 526 314 801 564 1175 257 430 1194 1516 1225 364 1375 960 144 647 821 937 371 833 1392 167 1038 292 879 753 15 1469